Veo Observer Plus Instructions d'exploitation

Thermo Scientific Dionex Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions (Original Operating Instructions) Revision

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 2 Operating Instructions Trademarks Empower is a registered trademark of Waters Corp. P

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 92 Operating Instructions Quick Troubleshooting Check The following guidelines can be u

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 93 7.2 Self-Test Error Codes Internal self-test diagnostics are

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 94 Operating Instructions Error Code Description 200 The detector failed to reach a s

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 95 7.3 Warning and Error Codes Each time a fault or error occur

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 96 Operating Instructions Warning Code Warning Message Description and Remedial Actio

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 97 Error Code Error Message Description and Remedial Action 29

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 98 Operating Instructions Error Code Error Message Description and Remedial Action 29

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 99 7.4 Operating Problems The following table provides informat

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 100 Operating Instructions Problem Probable Cause Remedial Action The system has very

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 101 Problem Probable Cause Remedial Action High baseline drift

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 3 1.2 Safety The CE Mark label and cTUVus Mark safety label on

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 102 Operating Instructions Problem Probable Cause Remedial Action High noise, non-per

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 103 Problem Probable Cause Remedial Action Spikes Electrical

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 104 Operating Instructions Problem Probable Cause Remedial Action Loss of response (C

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 105 Problem Probable Cause Remedial Action Poor peak area prec

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 106 Operating Instructions Problem Probable Cause Remedial Action Noisy baseline, hig

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 107 8 Maintenance 8.1 Safety Guidelines for Maintenance The f

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 108 Operating Instructions 8.2 Returning the Detector for Repair Before returning the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 109 8.3 Routine and Preventive Maintenance 8.3.1 Inspection an

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 110 Operating Instructions General Routine Maintenance in an LC System Perform the main

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 111 8.3.2 Maintaining the Detector between Analyses Prevent bui

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 4 Operating Instructions Warning: Indicates that failure to take note of the accompa

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 112 Operating Instructions 8.4 Eliminating Leakage The leak sensor is installed on the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 113 8.5 Replacing the Gas Filters The detector filters incoming

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 114 Operating Instructions 3. Carefully move the cover plate away from the detector en

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 115 8.6 Removing the Nebulizer Important: Even minute partic

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 116 Operating Instructions 8.7 Stream-Switching Valve (Corona Veo RS only) Tip: Whe

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 117 8.7.2 Assembling the Valve 1. Insert the rotor in the valv

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 118 Operating Instructions 8.8 Replacing the Main Power Fuses Warning: Turn off the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 119 8.9 Updating the Detector Firmware The detector is shipped

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 120 Operating Instructions 4. On the General page (→ page 81), the firmware version pr

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 121 9 Technical Information Specification Corona Veo Corona V

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 5 • Hazardous gases Install the HPLC system in a well-ventilate

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 122 Operating Instructions Specification Corona Veo Corona Veo RS Emission sound pres

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 123 10 Accessories, Consumables, and Spare Parts Accessories, s

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 124 Operating Instructions Description Part no. Quantity in the accessories kit Cable

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 125 Description Part no. Quantity in the accessories kit Nut a

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 126 Operating Instructions 10.2 Optional Accessories Accessories Description Part no

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 127 10.3 Consumables and Spare Parts The part number always ref

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 128 Operating Instructions Nebulizer Description Part no. Nebulizer, FocusJet, for Cor

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 129 11 Appendix 11.1 Digital I/O Pin Assignment The four TTL

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 130 Operating Instructions Important: When you connect the TTL inputs, ensure that t

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 131 Relay Outputs The "Pump Off" output contact is use

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 6 Operating Instructions • Always replace blown fuses with original spare part fuses a

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 132 Operating Instructions 11.2 Internal Gas and Aerosol Flow Path Diagram The followi

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 133 12 Index A Accessories Optional ...

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 134 Operating Instructions G Gas Connections ...

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 135 Stream-Switching Valve ...

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 136 Operating Instructions

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 7 1.2.3 Consignes de Sécurité Si vous utilisez d'instrumen

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 8 Operating Instructions • Gaz dangereux Installez le système HPLC dans un laboratoire

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 9 • Quand les capots de protection de l’appareil sont démontés,

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 10 Operating Instructions

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 11 1.3 Intended Use The device is designed to be operated only

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 12 Operating Instructions If there is a question regarding appropriate usage, contact T

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 13 1.4 Federal Communications Commission (FCC) Note This equipm

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 14 Operating Instructions

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 15 2 Overview 2.1 Unit Description The detector is a modern hi

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 16 Operating Instructions 2.2 Detector Configurations The detector is available in the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 17 2.3 Operating Principle The operating principle of the detec

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 18 Operating Instructions In the ion trap excess charge is removed. The charge of the r

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 19 2.4 Interior Front Panel The detector is designed to provid

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 20 Operating Instructions 2.5 Rear Panel Fig. 3: Rear Panel (here: Corona Veo RS) No.

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 21 2.6 Flow Connections The detector is designed to provide eas

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page I Declaration of Conformity (Original Declaration of Conformity)

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 22 Operating Instructions 2.10 Leak Sensor A leak sensor is located within the drip tr

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 23 3 Installation 3.1 Facility Requirements In addition to the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 24 Operating Instructions • Connect the detector to an electrical line that shares a c

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 25 Gas Supply Requirements Important: To prevent damage to th

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 26 Operating Instructions 3.2 Unpacking the Detector All electrical components of the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 27 3.3 Positioning the Detector in an UltiMate 3000 System If t

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 28 Operating Instructions Systems with Series and Parallel Detector Configuration The d

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 29 3.4 Connecting the Detector Rear Panel 3.4.1 Overview of Co

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 30 Operating Instructions 3.4.3 Connecting the USB Cable Connect the detector to the d

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 31 3.4.4 Connecting the Digital I/O General Information The de

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page II Operating Instructions

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 32 Operating Instructions For further information about connecting an UltiMate 3000 pum

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 33 4 Preparation for Operation (Startup) 4.1 Overview of Acti

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 34 Operating Instructions 4.2 Connecting the Drainage The detector has two drain port

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 35 4.3 Connecting the Gas Supply and Exhaust Tubing Connect the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 36 Operating Instructions 4.4 Making Flow Connections The following section provides i

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 37 4.4.2 Capillary Connections in an UltiMate 3000 System Note

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 38 Operating Instructions 4.4.3 Installing the In-Line Filter (optional) An in-line fi

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 39 4.4.4 Connecting Capillaries to the Detector To connect the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 40 Operating Instructions 4.4.5 Connecting the Stream-Switching Valve (Corona Veo RS o

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 41 4.5 General Guidelines for Detector Operation The following

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page i Table of Contents 1 Introduction ...

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 42 Operating Instructions The following table is to assist you with typical additives a

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 43 4.5.4 Ventilation Important: Volatile hydrocarbons such a

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 44 Operating Instructions

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 45 5 Operation 5.1 Safety Guidelines for Operation English S

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 46 Operating Instructions French Safety Guidelines Important: Lors de l'exploit

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 47 5.2 Turning on the Power to the Detector Before powering up

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 48 Operating Instructions 5.3 Operating the Detector from the Touch Screen 5.3.1 Over

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 49 5.3.2 Main Menu The Main Menu provides the serial number of

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 50 Operating Instructions 5.3.3 Run Mode Menu From the Main Menu, press the Run Mode s

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 51 Corona Veo RS only If the stream-switching valve is not set t

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page ii Operating Instructions 4.4.5 Connecting the Stream-Switching Valve (Corona Veo RS o

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 52 Operating Instructions 5.3.3.1 Diagnostics Screen The Diagnostics screen displays i

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 53 5.3.3.2 Graph Screen The Graph screen displays the online de

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 54 Operating Instructions 5.3.3.3 Evaporation Temperature Screen The Evaporation Tempe

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 55 5.3.4 System Setup Menu The System Setup Menu is used to edi

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 56 Operating Instructions 5.3.4.1 Gas Regulator Screen The Gas Regulator screen provid

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 57 5.3.4.2 Date & Time Setup Screen Access the Date & T

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 58 Operating Instructions 5.3.4.3 Contacts & Inputs Screen The Contacts & Inpu

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 59 5.4 Before Operating the Detector 5.4.1 Setting the Gas Pre

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 60 Operating Instructions 2. If applicable In the Run Mode Menu, select the Exit soft

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 61 5. Select Setpoint and set the pressure set point to the des

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page iii 6.3 Operating the Detector from Chromeleon ...

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 62 Operating Instructions 5.4.3 Equilibrating the Detector After you have prepared the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 63 The following table is to assist you with typical flow rates

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 64 Operating Instructions 5.5 Performing Sample Analysis This section provides informa

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 65 5.6 Optimizing the Detector Performance The performance of

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 66 Operating Instructions 5.6.2 Setting a Filter Constant The filter time constant is

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 67 Factor Evap. Temp. Guidelines Effect Corona Veo Corona Veo R

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 68 Operating Instructions 5.6.5 Applying a Power Function Value The signal of the dete

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 69 5.6.7 Digital Data Collection Rate Guidelines When you opera

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 70 Operating Instructions 5.7 Internal Safety Features 5.7.1 Leak Detection When a le

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 71 5.7.3 Gas Supply Pressure Relief Valve A pressure relief val

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page iv Operating Instructions

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 72 Operating Instructions 5.7.4 Flow Ratio Alarm The detector continuously monitors th

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 73 • Corona Veo RS: The stream-switching valve will actuate and

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 74 Operating Instructions 5.8 Shutting Down the Detector 5.8.1 Short-term Shutdown If

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 75 10. If you prepare the detector for shipment a) Remove the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 76 Operating Instructions

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 77 6 Chromeleon Software The detector can be controlled by the

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 78 Operating Instructions 6.1 Setting Up the Detector in Chromeleon This section provi

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 79 d) Turn on the detector power. Windows will now detect the de

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 80 Operating Instructions 6.1.2 Installing the Detector The detector should complete

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 81 6.1.3 Configuring the Detector 6.1.3.1 Initial Installation

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 1 1 Introduction 1.1 How to Use This Manual The layout of this

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 82 Operating Instructions In the virtual mode, Chromeleon simulates detector control an

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 83 • Device Name Displays the name used to identify the detecto

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 84 Operating Instructions 6.1.3.2 Changing the Configuration Properties You may reopen

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 85 6.3 Operating the Detector from Chromeleon Before you begin

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 86 Operating Instructions 6.3.2 Direct Control With direct control, you select operati

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 87 To open a control panel 1. On the View menu, click Default P

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 88 Operating Instructions 6.3.3 Automated Control With automated control, you create a

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 89 2. Change the settings in the program as desired. The easies

Charged Aerosol Detectors Corona Veo and Corona Veo RS Page 90 Operating Instructions

Charged Aerosol Detectors Corona Veo and Corona Veo RS Operating Instructions Page 91 7 Troubleshooting 7.1 Overview The following features help